Comprehensive UHPLC-MS screening methods for the analysis of triazolopyrazine precursor and its genotoxic nitroso-derivative in sitagliptin pharmaceutical formulation-论文-万方医学网

Comprehensive UHPLC-MS screening methods for the analysis of triazolopyrazine precursor and its genotoxic nitroso-derivative in sitagliptin pharmaceutical formulation

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作者： Jires, Jakub ^[1] ; Dousa, Michal ^[2] ; Gibala, Petr ^[3] ; Doubsky, Jan ; Pecek, Daniel ; Mervart, David ; Kluk, Anna ; Veseli, Ardita ; Kalasek, Stanislav ; Rezanka, Pavel

作者单位： Department of Analytical chemistry, Faculty of Chemical Engineering, UCT Prague, Technicka ′ 5 ^[1] Praha ^[2] PrahaUniv Ljubljana Fac Pharm Dept Biopharmaceut & Pharmacokinet ^[3]

关键词 Sitagliptin Nitrosation Nitrites Scavengers NTTP Triazolopyrazine INHIBITOR EFFICIENT PRODUCTS

发布时间 2024-04-11

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Comprehensive UHPLC-MS screening methods for the analysis of triazolopyrazine precursor and its genotoxic nitroso-derivative in sitagliptin pharmaceutical formulation

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Comprehensive UHPLC-MS screening methods for the analysis of triazolopyrazine precursor and its genotoxic nitroso-derivative in sitagliptin pharmaceutical formulation

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