换一批
第一作者：
Amgad M,Rabie
第一单位：
Department of Pharmaceutical Organic Chemistry, Faculty of Pharmacy, Mansoura University, Mansoura 35516, Egypt.
作者：
关键词
(Compounds: 3,4,5-Trihydroxybenzohydrazide (galloyl hydrazide, target compound, coded as 2nz) and Ethyl 3,4,5-trihydroxybenzoate (ethyl gallate, intermediate compound, coded as 1nz)3,4,5-TrihydroxybenzohydrazideACN, acetonitrileAbs., absoluteAq, aqueousArom., aromaticChemical Transformation (esterification and hydrazinolysis reactionsConc., concentratedConv., conventionalDEE, diethyl etherEtOAc, ethyl acetateEtOH, ethanolEthyl gallateGalloyl hydrazideM.P., melting pointM.Wt., molecular weightMS, mass spectrometryMW, microwaveMWI, microwave irradiationMeOH, methanolMicrowave-assisted synthesisPet., petroleumR.T., room temperatureRP, reversed-phaseRecryst., recrystallizedRel. Int., relative intensityRotavap, rotary evaporatorS, singletSpectroscopic analysesStr., strongT.D.S., triple distribution systemTFA, trifluoroacetic acidTMS, tetramethylsilaneV/v, volume per volumeV/v/v, volume per volume per volumeXss., excesssynthesis using both conventional heating and one-pot solventless greener microwave heating techniques) followed by Complete Purification and Full Elucidative Characterization (chromatographic, physicochemical, spectroscopic, and elemental characterization for identification)
DOI
10.1016/j.mex.2019.11.010
PMID
32025504
发布时间
2020-09-28
- 浏览2
MethodsX
2020年7卷
100737页
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