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首页> Journal of pharmaceutical and biomedical analysis> Rapid and sensitive LC-MS/MS method for the enantioanalysis of verapamil in rat plasma using superficially porous silica isopropyl-cyclofructan 6 chiral stationary phase after SPE: Application to a stereoselective pharmacokinetic study.

Rapid and sensitive LC-MS/MS method for the enantioanalysis of verapamil in rat plasma using superficially porous silica isopropyl-cyclofructan 6 chiral stationary phase after SPE: Application to a stereoselective pharmacokinetic study.

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作者： Mohamed,Hefnawy ^[1] ; Abdulrhman,Al-Majed ^[2] ; Haitham,Alrabiah ^[2] ; Nasser,Algrain ^[2] ; Mostafa,Mohammed ^[3] ; Yousef Bin,Jardan ^[4]

作者单位： Department of Pharmaceutical Chemistry, College of Pharmacy, King Saud University, P. O. Box 2457, Riyadh, 11451, Saudi Arabia; Department of Analytical Chemistry, Faculty of Pharmacy, Mansoura University, Mansoura, 35516, Egypt. Electronic address: mhefnawy@ksu.edu.sa. ^[1] Department of Pharmaceutical Chemistry, College of Pharmacy, King Saud University, P. O. Box 2457, Riyadh, 11451, Saudi Arabia. ^[2] Department of Pharmaceutical Chemistry, College of Pharmacy, King Saud University, P. O. Box 2457, Riyadh, 11451, Saudi Arabia; National Organization for Drug Control and Research, P.O. Box 29, Cairo, Egypt. ^[3] Department of Pharmaceutics, College of Pharmacy, King Saud University, P. O. Box 2457, Riyadh, 11451, Saudi Arabia. ^[4]

关键词 LC–MS/MS Pharmacokinetics Rat plasma Solid-phase extraction Superficially porous silica isopropyl-cyclofructan chiral column Verapamil enantiomers

主题词动物(Animals);色谱法, 液相(Chromatography, Liquid);果聚糖类(Fructans);多孔性(Porosity);大鼠(Rats);结果可重复性(Reproducibility of Results);二氧化硅(Silicon Dioxide);固相萃取(Solid Phase Extraction);立体异构现象(Stereoisomerism);串联质谱法(Tandem Mass Spectrometry);维拉帕米(Verapamil)

DOI 10.1016/j.jpba.2021.114108

PMID 33962179

发布时间 2021-06-17

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Journal of pharmaceutical and biomedical analysis

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