Separation of menaquinone-7 geometric isomers by semipreparative high-performance liquid chromatography with silver complexation and identification by nuclear magnetic resonance.

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作者： Katarzyna,Bus ^[1] ; Jerzy,Sitkowski ^[2] ; Wojciech,Bocian ^[2] ; Adam,Zmysłowski ^[1] ; Karol,Ofiara ^[1] ; Arkadiusz,Szterk ^[3]

作者单位： National Medicines Institute, Department of Spectrometric Methods, 30/34 Chełmska, 00-725 Warsaw, Poland. ^[1] National Medicines Institute, Counterfeit Medicinal Products and Designer Drugs Department, 30/34 Chełmska, 00-725 Warsaw, Poland. ^[2] Center for Translationale Medicine Warsaw University for Life Sciences, Nowoursynowska 100, 02-797 Warsaw, Poland; Instytut Innowacji Przemysłowych MAT, 3/63 Rabindranatha Tagore, 02-647 Warsaw, Poland. Electronic address: ^[3] 20szterkarkadiusz@gmail.com. ^[4]

关键词 Argentation chromatography Density functional theory Dietary supplement Geometric isomer Menaquinone-7 Nuclear magnetic resonance Vitamin K2

主题词色谱法, 高压液相(Chromatography, High Pressure Liquid);磁共振波谱学(Magnetic Resonance Spectroscopy);银(Silver);维生素K2(Vitamin K 2)

DOI 10.1016/j.foodchem.2021.130890

PMID 34438182

发布时间 2022-06-14

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