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Sensitive quantitation of ultra-trace toxic aconitines in complex matrices by perfusion nano-electrospray ionization mass spectrometry combined with gas-liquid microextraction.

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第一作者： Zidong,Qiu

第一单位： State Key Laboratory for Quality Ensurance and Sustainable Use of Dao-di Herbs, National Resource Center for Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing, 100700, China. Electronic address: qiuzidong@126.com.

作者： Zidong,Qiu ^[1] ; Chaofa,Wei ^[2] ; Liping,Kang ^[2] ; Li,Zhou ^[2] ; Changjiangsheng,Lai ^[2] ; Xiang,Li ^[2] ; Binbin,Yan ^[2] ; Jiaquan,Xu ^[3] ; Shuanglong,Wang ^[4] ; Luqi,Huang ^[5]

作者单位： State Key Laboratory for Quality Ensurance and Sustainable Use of Dao-di Herbs, National Resource Center for Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing, 100700, China. Electronic address: qiuzidong@126.com. ^[1] State Key Laboratory for Quality Ensurance and Sustainable Use of Dao-di Herbs, National Resource Center for Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing, 100700, China. ^[2] Jiangxi Key Laboratory for Mass Spectrometry and Instrumentation, College of Chemistry, Biology and Material Sciences, East China Institute of Technology, Nanchang, 330013, China. ^[3] Jiangxi Key Laboratory for Mass Spectrometry and Instrumentation, College of Chemistry, Biology and Material Sciences, East China Institute of Technology, Nanchang, 330013, China. Electronic address: jiayou1010@163.com. ^[4] State Key Laboratory for Quality Ensurance and Sustainable Use of Dao-di Herbs, National Resource Center for Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing, 100700, China. Electronic address: huangluqi01@126.com. ^[5]

关键词 Aconitum Complex matrices Gas-liquid microextraction Perfusion nano-electrospray ionization mass spectrometry Ultra-trace analysis

医学主题词乌头碱(Aconitine);色谱法, 高压液相(Chromatography, High Pressure Liquid);光谱法, 质量, 电喷雾电离(Spectrometry, Mass, Electrospray Ionization);生物碱类(Alkaloids);灌流(Perfusion);乌头属(Aconitum);质量控制(Quality Control)

DOI 10.1016/j.talanta.2023.125402

PMID 37979510

发布时间 2024-01-16

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