摘要Amides can be obtained in good to excellent yield by Sm/TiCl4 mediated reductive cleavage of N=N bond in azo compounds and successive acylation in one pot. It offers an alternative method for the synthesis of amides from very simple starting materials directly.
作者单位Department of Chemistry, Zhejiang University, Hangzhou 310028, China[1]Department of Chemistry, Zhejiang University, Hangzhou 310028, China;State Key Laboratory of Organometallic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China[2]